HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethyl-1,3-propanediamine → HCID 178483529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethyl-1,3-propanediamine | HCID 7993 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl- | HCID 4712192 | — |
| Product | HCID 178483529 | HCID 178483529 | 26% |
Reaction Steps
Prepared as in Example 1 from 2-benzoyl-benzo[b]-thiophen-3-ol, phosphorus(V) chloride and an aqueous solution of 3-(dimethylamino)-propylamine (prepared from 51 gm of diamine and 70 cc of water) with a yield of 26% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288437 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-dc9ea1c034544dd480f57af891e476c3 |
| Source note | uspto-grants-1981_09 |