HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 178457124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl- | HCID 4712192 | — |
| Product | HCID 178457124 | HCID 178457124 | 54% |
Reaction Steps
Prepared as in Example 1 from 2-benzoyl-benzo[b]thiophen-3-ol, phosphorus(V) chloride and an aqueous 38.5% isopropylamine solution with a yield of 54% of theory. M.P. 112°-113° C. (ethyl acetate/petroleum ether 1:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288437 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-e0788fceaf0b4eb5996681857f85280e |
| Source note | uspto-grants-1981_09 |