Cyclohexylamine → HCID 178516386, compound

HRID 1577548Notes

Reaction equation

HRID 1577548 reaction equation
[C:1]([C:9]1[S:13][C:12]2[CH:14]=[CH:15][CH:16]=[CH:17][C:11]=2[C:10]=1[OH:18])(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:19]1([NH2:25])[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>>[CH:19]1([NH:25]/[C:1](/[C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)=[C:9]2\[C:10](=[O:18])[C:11]3[CH:17]=[CH:16][CH:15]=[CH:14][C:12]=3[S:13]\2)[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1

Participants

3

Reactant 2

HCID 7965CyclohexylamineHCID 4712192Methanone, (3-hydroxybenzo[b]thien-2-yl)phenyl-

Product 1

HCID 178516386HCID 178516386, compoundYield 56%

Procedure

Prepared as in Example 31 with a yield of 56% of theory from 2-benzoyl-benzo[b]thiophen-3-ol and cyclohexylamine. Lemon-yellow crystals were obtained, m.p. 122°-123° C. (petroleum ether/ethyl acetate 85:15).

Workup

  1. customLemon-yellow crystals were obtained

Sources & evidence

ORD record
ord-13e1cf20a2e24171b132b3bab00a0343
Source dataset
uspto-grants-1981_09
Patent number
US04288437

Reaction notes

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