HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → Acetanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Acetanilide | HCID 904 | — |
Reaction Steps
Acetanilide is prepared by the method of Example 5 using 5.0 mls (0.05 mole) of aniline, 7.5 grams of 3A molecular sieves and 6.6 g (0.065 mole) of acetic anhydride in 100 mls of methylene chloride. The crude product (6.23 grams; 86% of theoretical) is recrystallized from toluene to obtain pure acetanilide, m.p. 112°-114° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288592 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-65be4125e5164f78aba0f46d43f4f0ba |
| Source note | uspto-grants-1981_09 |