HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20571322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Methoxyethanol | HCID 8019 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Methyl 3,5-dichloro-4-hydroxybenzoate | HCID 76856 | — |
| Reactant | 1,2,3,5-Tetrabromo-4,6-bis(bromomethyl)benzene | HCID 14419177 | — |
| Product | HCID 20571322 | HCID 20571322 | — |
Reaction Steps
In a four-liter reaction vessel, 3 liters of methyl glycol (B.P. 122°-126° C.), 221 g (1 mole) of 3,5-dichloro-4-hydroxybenzoic acid methyl ester, 40 g (1 mole) of sodium hydroxide in 40 ml of water, and 289.8 g (0.5 mole) of 1,3-bis-(bromomethyl)-2,4,5,6-tetrabromobenzene were reacted and worked up in the manner described in Example 46.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04288607 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-d3c15417da5f43a1a3f617fa0c13999f |
| Source note | uspto-grants-1981_09 |