HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20568783, compound → HCID 20518074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20568783 | HCID 20568783 | — |
| Solvent | 1-Pentanol | HCID 6276 | — |
| Product | HCID 20518074 | HCID 20518074 | 184.5% |
Reaction Steps
The procedure described in Example (1b) is repeated, using 52.3 g (0.193 mole) of 2,2-dimethyl-11-aminoundecanoic acid and 200 ml of n-pentanol. Distillation yields 60.5 g (0.178 mole) of 2,2-dimethyl-11-isopropyl-11-aminoundecanoic acid pentyl ester, corresponding to a yield of 92.2% of theory: b.p. 138°-139°/0.01 torr; nD20 =1.4505.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04290964 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-94f5740ce59e4041a446807c1d242142 |
| Source note | uspto-grants-1981_09 |