Benzyl Chloride → HCID 178475086, compound

Participants

Reaction Steps

5.2 g (0.02 M) of N-(2,6-dichlorophenyl)-N'-acetyl-thiourea, 1.7 g of (0.012 M) of ground potassium carbonate 2.6 ml (0.024 M) of benzylchloride and 80 ml of acetone are boiled in a reflux being energetically shaken for 4 hours. The acetone is distilled off. The product in the flask is washed with water and is filtered. After drying N-(2,6-dichlorophenyl)-N'-acetyl-S-benzylisothiourea is obtained with a melting point of 84°-95° C. After being recrystallized twice from ethanol it has a melting point of 99°-101° C., whereby 1.7 g are isolated (24% of the theoretical yield).

Provenance & Evidence