N,N-Dimethyl-1,3-propanediamine → HCID 135601370, compound

Participants

Reaction Steps

By following the procedure of Example 3, and using 7-chloro-2-methyl-3-[4-(trifluoromethyl)phenyl]-3,4-dihydro-1,9(2H,10H)-acridinedione instead of 7-chloro-3-(3,4-dichlorophenyl)-3,4-dihydro-1,9(2H,10H)acridinedione and N,N-dimethyl-1,3-propanediamine instead of N,N-diethylenediamine one obtains 7-chloro-1-[[3-(dimethylamino)propyl]imino]-1,3,4,10-tetrahydro2-methyl-3-[4-(trifluoromethyl)phenyl]-9(2H)-acridinone; mp 169°-170° C. after chromatography on silica eluted with chloroform/methanol 7:1.

Provenance & Evidence