HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethylaniline → HCID 22973868, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethylaniline | HCID 6896 | — |
| Reactant | Methyl pyruvate | HCID 11748 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 22973868 | HCID 22973868 | — |
Reaction Steps
A solution of 2,6-dimethyl aniline (37.2 ml; 0.3 mol) in benzene (200 ml) was added with 0.5 g of ZnCl2 and, dropwise at room temperature, with 33.2 ml (0.33 mol) of methyl pyruvate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04291049 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-36bdfb12a1574d90bf1c157b223fc447 |
| Source note | uspto-grants-1981_09 |