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HRID1578126

反应详情

EQUATION

反应方程式

HRID 1578126 的结构方程式

REACTANTS

反应物

3
结构：c1ccncc1
HCID1049

Pyridine

C5H5N

结构：CC(C)=CC1C(C(=O)Cl)C1(C)C
HCID26620

2,2-Dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropane-1-carbonyl chloride

C10H15ClO

结构：N#CC(O)c1cccc(OC=C(Cl)Cl)c1
HCID20568925

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)=CC1C(C(=O)OC(C#N)c2cccc(OC=C(Cl)Cl)c2)C1(C)C
HCID54357514

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

2 次

PROCEDURE

实验过程

To a solution of 9.8 g of 3-(2,2-dichlorovinyloxy)-mandelonitrile and 7.5 g of 2,2-dimethyl-3-(1-isobutenyl)-cyclopropanecarboxylic acid chloride in 100 cc toluene is added a solution of 3.5 g of pyridine in 200 ml toluene dropwise within 10 minutes. The resultant suspension is stirred for 15 hours at 20°-25° C., washed with dilute HCl and totally concentrated.

WORKUP

后处理

  1. washwashed with dilute HCl
  2. concentrationtotally concentrated