HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1578249Generated: November 2, 2026
HCID 13469073, compound → HCID 54070603, compound
https://huagongshe.com/reaction/1578249
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 13469073 | HCID 13469073 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 54070603 | HCID 54070603 | — |
Reaction Steps
248 mg (0.6 m mol) of 1α,3β-dihydroxy-24-oxo cholesta-5,7-dien and 101 mg (0.9 m mol) of potassium-t-butoxide was dissolved in a mixture of t-butyl alcohol and ethyleneglycol dimethyl ether (1:1 V/V) warming at 40° C., and while cooling the solution with icewater to about 0° C. and stirring violently.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04292249 |
|---|
| Source dataset | uspto-grants-1981_09 |
|---|
| ORD ID | ord-863f9890ce2c497f9a9a540cdeb13b91 |
|---|
| Source note | uspto-grants-1981_09 |
|---|
