HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → 3-[N-phenyl-N-(4-nitrophenyl)amino]-1-bromopropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | Propanoyl chloride, 3-bromo- | HCID 84944 | — |
| Reactant | 3-[N,N-diphenylamino)-1-bromopropane | HCID 10827329 | — |
| Reactant | N-phenyl-N-(4-nitrophenyl)amide | HCID 86738022 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-[N-phenyl-N-(4-nitrophenyl)amino]-1-bromopropane | HCID 20482619 | — |
Reaction Steps
3-[N-phenyl-N-(4-nitrophenyl)amino]-1-bromopropane is prepared from N-phenyl-N-(4-nitrophenyl)amide with 3-bromopropionyl chloride, followed by reduction with borane in tetrahydrofuran, by a procedure analogous to the preparation of 3-[N,N-diphenylamino]-1-bromopropane in Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04292321 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-fbe1168b47914c31979f254b089ef0ec |
| Source note | uspto-grants-1981_09 |