HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → 3-(N,N-diphenylamino)-1-chloropropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | Diphenylamine | HCID 11487 | — |
| Reactant | 3-Chloropropionyl chloride | HCID 69364 | — |
| Reactant | 3-[N,N-diphenylamino)-1-bromopropane | HCID 10827329 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-(N,N-diphenylamino)-1-chloropropane | HCID 10658053 | — |
Reaction Steps
3-(N,N-diphenylamino)-1-chloropropane is prepared by the reaction of diphenylamine with 3-chloropropionyl chloride, followed by reduction with borane in tetrahydrofuran, by a procedure analogous to the preparation of 3-[N,N-diphenylamino]-1-bromopropane in Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04292321 |
| Source dataset | uspto-grants-1981_09 |
| ORD ID | ord-a3e5be02d1d2492f8050a7b075ed5a73 |
| Source note | uspto-grants-1981_09 |