HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → Oxazolidine, 2,2,4,4-tetramethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | 2-Amino-2-methyl-1-propanol | HCID 11807 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Oxazolidine, 2,2,4,4-tetramethyl- | HCID 641504 | 57% |
Reaction Steps
Firstly, the precursor compound (2,2,4,4-tetramethyl-1,3-oxazolidine was prepared. To 237 g (3.0 mole) of 2-amino-2-methyl-1-propanol, there was added approximately 750 ml of dry benzene containing 174 g (3.0 mole) of acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03936466 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-5f36242c94644883938fad8b86f7ef6d |
| Source note | uspto-grants-1976_02 |