HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 20365142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Lithium | HCID 3028194 | — |
| Reactant | HCID 20365138 | HCID 20365138 | — |
| Product | HCID 20365142 | HCID 20365142 | — |
Reaction Steps
A sample of 1-methyl-α-(2-methylphenyl)-3-pyrrolidineethanol (23 g, 0.105 moles) is subjected to Birch reduction in 500 ml liquid ammonia with 7 g (1 mole) of lithium to give a quantitative yield of 3-(3,6-dihydro-2-methylphenethyl)-N-methylpyrrolidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03936465 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-3d3fbf24c2a74d58a23bf1625e5eea9e |
| Source note | uspto-grants-1976_02 |