Glycidyl methacrylate → Methacryloyloxyhydroxypropyl methyl octadecyl amine

HRID 1578420노트

반응식

HRID 1578420 반응식
[CH3:1][NH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].[C:21]([O:26]CC1OC1)(=[O:25])[C:22]([CH3:24])=[CH2:23]>CO>[C:21]([O:26][CH:3]([N:2]([CH2:23][CH2:22][CH2:21][OH:25])[CH3:1])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20])(=[O:25])[C:22]([CH3:24])=[CH2:23]

참가 물질

4

반응물 2

HCID 7837Glycidyl methacrylateHCID 75539N-Methyloctadecylamine

생성물 1

HCID 86733040Methacryloyloxyhydroxypropyl methyl octadecyl amine

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

Equimolar quantities of N-methyl-N-octadecyl amine and glycidyl methacrylate were reacted together in methanol to form methacryloyloxyhydroxypropyl methyl octadecyl amine. 14.3 grams of the resultant amine were dissolved in 20 grams of dimethyl formamide and 4.2 grams of dimethyl sulfate were added slowly with stirring. After 10 days' standing at 25°C, 9 grams of crystalline material was isolated, washed with ether, and dried. The sulfate band in the crystalline product was identified in the I.R. spectrum.

출처 및 근거

ORD 기록
ord-9109ef3dd74f49acbf478860b132f8d5
출처 데이터셋
uspto-grants-1976_02
특허 번호
US03936492

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