Acrylonitrile → HCID 68133413, compound

HRID 1578426Notes

Reaction equation

HRID 1578426 reaction equation
[C:1](#[N:4])[CH:2]=[CH2:3].[C:5]1([CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][NH2:29])[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1>O>[C:1]([CH2:2][CH2:3][NH:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][C:5]1[CH:6]=[CH:7][CH:8]=[CH:9][CH:10]=1)#[N:4]

Participants

4

Reactant 2

HCID 7855AcrylonitrileHCID 19801454HCID 19801454, compound

Product 1

HCID 68133413HCID 68133413, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

N-(Beta-cyanoethyl)phenyloctadecylamine was prepared as follows: Acrylonitrile (61.0 grams, 1.15 moles) was added slowly over 2 hours, with stirring, to a mixture of phenyloctadecylamine, prepared as described in Example II, (363.8 grams, 1.05 moles) and 17.0 grams water at 60°-70°C. The resulting mixture was then stirred at 70°-80° for 4 additional hours. The water was separated and the product dried under reduced pressure at 60°-70°C.

Workup

  1. customprepared
  2. customThe water was separated
  3. customthe product dried under reduced pressure at 60°-70°C.

Sources & evidence

ORD record
ord-360c00477d85493bb412146981af4679
Source dataset
uspto-grants-1976_02
Patent number
US03936503

Reaction notes

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