Sodium Hydroxide → 2-Propanol, 2-[(1,1-dimethylethyl)azo]-

HRID 1578578Notes

Reaction equation

HRID 1578578 reaction equation
[OH-:1].[Na+].[C:3]([N:7]=[N:8][C:9](Cl)([CH3:11])[CH3:10])([CH3:6])([CH3:5])[CH3:4]>C(O)(C)(C)C>[C:3]([N:7]=[N:8][C:9]([OH:1])([CH3:11])[CH3:10])([CH3:6])([CH3:5])[CH3:4]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 1564434955296-56-5

Product 1

HCID 945822-Propanol, 2-[(1,1-dimethylethyl)azo]-

Reagents, catalysts & solvents 1

HCID 6386tert-ButanolSolvent

Procedure

2-t-butylazo-2-hydroxypropane was prepared by reacting aqueous sodium hydroxide and 2-t-butylazo-2-chloropropane in t-butyl alcohol. The 2-t-butylazo-2-hydroxypropane was isolated by diluting the alcohol solution with water and extracting with pentane.

Workup

  1. custom2-t-butylazo-2-hydroxypropane was prepared

Sources & evidence

ORD record
ord-bdfc4ee1dfb24fed9dd905887676dae0
Source dataset
uspto-grants-1976_02
Patent number
US03937761

Reaction notes

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