HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3,5-Bis(benzyloxy)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3,5-Bis(phenylmethoxy)benzoic acid | HCID 99307 | — |
| Product | 3,5-Bis(benzyloxy)benzoyl chloride | HCID 10831869 | — |
Reaction Steps
167 g of 3,5-dibenzyloxybenzoic acid and 400 ml of redistilled thionyl chloride were refluxed on an oil bath for 1 hour. Excess thionyl chloride was distilled off at reduced pressure, and the remaining mass crystallized. The product was recrystallized from petroleum ether (B.p., 60°-85°C.) : M.P. 73°-74°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03937838 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-25fdc2269fbc4de39071a3220be82b75 |
| Source note | uspto-grants-1976_02 |