HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine-1-propanol → HCID 86733061, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine-1-propanol | HCID 66032 | — |
| Reactant | HCID 12331791 | HCID 12331791 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86733061 | HCID 86733061 | — |
Reaction Steps
A solution of 12.8 g (0.044 mole) of dibenzofuran-2,8-dicarbonyl chloride and 12.6 g (0.088 mole) of 3-piperidinopropanol in 1 liter of chloroform is refluxed for 4 hours. Upon dilution with diethyl ether, the product is collected and crystallized from ethanol, to give bis(3-piperidinopropyl)dibenzofuran-2,8-dicarboxylate dihydrochloride monohydrate, M.P. 252°-253°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03937833 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-ab38c0313f1e462ca2c7c590761877e2 |
| Source note | uspto-grants-1976_02 |