HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 86733062, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 13587364 | HCID 13587364 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86733062 | HCID 86733062 | — |
Reaction Steps
A solution of 19.1 grams (0.1 mol) ethyl 2-chloroethylphosphonochloridate (from Example 2) in 200 ml. dry diethyl ether was cooled to 5°C. and a solution of 8.7 grams (0.1 mol) morpholine and 10.1 grams (0.1 mole) triethylamine in 100 ml. dry diethyl ether added dropwise. After stirring 1 hour at room temperature the amine hydrochloride was removed by filtration and washed with ether. The filtrate was freed of solvent by flash evaporation. The residue weighed 22.4 grams. ##EQU11##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03938983 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-12799d64c8bd4cfa9a64922d9db30272 |
| Source note | uspto-grants-1976_02 |