HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 68137482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Hexamethylphosphoramide | HCID 12679 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | Epicillin | HCID 71392 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68137482 | HCID 68137482 | — |
Reaction Steps
A mixture of 1 g. of epicillin, 0.5 g. of anhydrous magnesium sulfate, 0.7 ml. of triethylamine, and 5 ml. of hexamethylphosphoramide amide, and 25 ml. of dichloromethane was stirred for 30 minutes at room temperature and then magnesium sulfate was filtered off to provide a dichloromethane solution of epicillin triethylamine salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03939150 |
| Source dataset | uspto-grants-1976_02 |
| ORD ID | ord-7be407de97494cc3b93979b3030f46ae |
| Source note | uspto-grants-1976_02 |