HRID1578776

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID140230

未命名化合物

HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

PRODUCTS

生成物

结构：CCOC(=O)C1=C(N)NC(c2ccccc2)=C(C(=O)O)C1c1ccccc1

HCID70635527

未命名化合物

收率 48%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

Upon boiling a solution of 14.0 g of benzylidenebenzoylacetic acid ethyl ester and 6.5 g of amidinoacetic acid ethyl ester in 150 ml of ethanol for 2 hours, 2-amino-4,6-diphenyl-1,4-dihydropyridine-3,5-dicarboxylic acid ethyl ester of melting point 183°C (ethanol) is obtained.

WORKUP

后处理

customfor 2 hours