反应详情

A mixture of 0.2 g. of cobalt octoate and 70 g. of trioctyl phosphite is warmed in vacuo (10 mm.) at 30°C while oxygen is added over a period of six hours. The mixture is stirred throughout this period by means of a magnetic stirrer. The product is washed with an aqueous alkaline solution to remove the cobalt catalyst, having a 91% yield of trioctyl phosphate.

1. additionA mixture of 0.2 g
2. additionis added over a period of six hours
3. washThe product is washed with an aqueous alkaline solution
4. customto remove the cobalt catalyst