HCID 131710058, compound → HCID 21557324, compound

HRID 1578928Notes

Reaction equation

HRID 1578928 reaction equation
Cl.[CH3:2][C:3]([C:5]1[C:10]([C:11]2[CH:16]=[CH:15][C:14]([Cl:17])=[CH:13][CH:12]=2)=[C:9]([NH2:18])[N:8]=[C:7]([NH2:19])[N:6]=1)=[O:4]>O>[CH3:2][C:3]([C:5]1[C:10]([C:11]2[CH:12]=[CH:13][C:14]([Cl:17])=[CH:15][CH:16]=2)=[C:9]([NH2:18])[N:8]=[C:7]([NH2:19])[N:6]=1)=[O:4]

Participants

3

Reactant 1

HCID 131710058HCID 131710058, compound

Product 1

HCID 21557324HCID 21557324, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A sample of [2,6-diamino-5-(p-chlorophenyl)-4-pyrimidinyl] methyl ketone, hydrochloride was dissolved in water and then precipitated with concentrated NH4OH to give the title compound, m.p. 206°-208°.

Workup

  1. customprecipitated with concentrated NH4OH

Sources & evidence

ORD record
ord-dd58c6670d4f42e1bdc86e01ee2a3cab
Source dataset
uspto-grants-1976_02
Patent number
US03940393

Reaction notes

Loading…