HCID 178433992, compound → HCID 178433993, compound
Reaction equation
[CH3:1][C:2]1[NH:3][C:4]([C:7]2[N:8]([CH2:15]CO)[C:9]([N+:12]([O-:14])=[O:13])=[CH:10][N:11]=2)=[N:5][N:6]=1.OCCN1C([N+]([O-])=O)=CN=C1C(NNC(=O)C)=N>>[CH3:1][C:2]1[NH:3][C:4]([C:7]2[N:8]([CH3:15])[C:9]([N+:12]([O-:14])=[O:13])=[CH:10][N:11]=2)=[N:5][N:6]=1Participants
3
Procedure
Using the above procedure 2-(5-methyl-4H-1,2,4-triazol-3-yl)-1-(2-hydroxyethyl)-5-nitroimidazole (VI J) is prepared from 2-[1-(2-hydroxyethyl)-5-nitro-2-imidazolecarboximidoyl)-1-acetylhydrazine.
Sources & evidence
- ORD record
- ord-5142ecaa283e430685ca6ffd47e02b39
- Source dataset
- uspto-grants-1976_02
- Patent number
- US03940411
Reaction notes
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