Bromine → HCID 23344750, compound

Participants

Reaction Steps

1-t-Butylazo-1-cyano-3,3,5-trimethylcyclohexane was prepared by bromine oxidation of the above 1-t-butylhydrazo-1-cyano-3,3,5-trimethylcyclohexane in the same way that 4-t-butylhydrazo-4-cyano-2,6-dimethylheptane was oxidized in Example VIIC. The yield of liquid product was 8.2 g. (63%) and the infrared spectrum was consistent with the structure of the proposed compound.

Provenance & Evidence