HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Aminobenzoic Acid → 4-(1-Cyclohexene-1-carbonylamino)-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Aminobenzoic Acid | HCID 978 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Cyclohexenecarbonyl chloride | HCID 142066 | — |
| Product | 4-(1-Cyclohexene-1-carbonylamino)-benzoic acid | HCID 21486323 | — |
Reaction Steps
88.0%. B. 4-(1-cyclohexene-1-carbonylamino)-benzoic acid was prepared as described in Example 1 from 16.6 g (0.121 mol) of p-aminobenzoic acid with 22.0 g (0.152 mol) of 1-cyclohexene-1-carboxylic acid chloride and 21.3 ml (0.152 mol) of triethylamine. Recrystallization from THF/n-pentane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931153 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-1b4f930b1f344eb1bb37ea873bd3d194 |
| Source note | uspto-grants-1976_01 |