HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Sulfide → HCID 86732861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Sulfide | HCID 402 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21547219 | HCID 21547219 | — |
| Reactant | HCID 21547228 | HCID 21547228 | — |
| Reactant | HCID 21547261 | HCID 21547261 | — |
| Product | HCID 86732861 | HCID 86732861 | — |
Reaction Steps
By the procedures described in Example 9, α-(6-methyl-2-pyridyl)-2-propenol is treated with thionyl chloride, the resulting 2-(1-chloro-2-propenyl)-6-methylpyridine is reacted with sodium cyanide and the 2-(6-methyl-2-pyridyl)-3-butenenitrile is treated with hydrogen sulfide to give 2-(6-methyl-2-pyridyl)-3-thiobutenamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931162 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-08e26248c79c4ddc93599e996a2ad997 |
| Source note | uspto-grants-1976_01 |