Phenethyl bromide → HCID 13009320, compound
Reaction equation
[C:1]1([CH2:7][CH2:8]Br)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1(CCC[P:19]([Cl:21])[Cl:20])C=CC=CC=1>>[C:1]1([CH2:7][CH2:8][P:19]([Cl:21])[Cl:20])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1Participants
3
Procedure
This compound was prepared from 2-phenylethylbromide (230g, 1.24 mole) by the method described above for the preparation of 3-phenylpropylphosphonous dichloride. 2-Phenylethylphosphonous dichloride was obtained as a pungent colourless liquid (115g, 45%), b.p. 64-66 at 0.001 mm.
Sources & evidence
- ORD record
- ord-36146f1ceacf45e7b3fec54560219e22
- Source dataset
- uspto-grants-1976_01
- Patent number
- US03931196
Reaction notes
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