Phenethyl bromide → HCID 13009320, compound

HRID 1579307Notes

Reaction equation

HRID 1579307 reaction equation
[C:1]1([CH2:7][CH2:8]Br)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1(CCC[P:19]([Cl:21])[Cl:20])C=CC=CC=1>>[C:1]1([CH2:7][CH2:8][P:19]([Cl:21])[Cl:20])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

3

Procedure

This compound was prepared from 2-phenylethylbromide (230g, 1.24 mole) by the method described above for the preparation of 3-phenylpropylphosphonous dichloride. 2-Phenylethylphosphonous dichloride was obtained as a pungent colourless liquid (115g, 45%), b.p. 64-66 at 0.001 mm.

Sources & evidence

ORD record
ord-36146f1ceacf45e7b3fec54560219e22
Source dataset
uspto-grants-1976_01
Patent number
US03931196

Reaction notes

Loading…