HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20560070, compound → HCID 20559963, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20560070 | HCID 20560070 | — |
| Reactant | 1-Methyl-2-[2-(2-nitrophenyl)ethenyl]pyridin-1-ium iodide | HCID 66760442 | — |
| Product | HCID 20559963 | HCID 20559963 | — |
Reaction Steps
Reduction of 2-(o-formamidophenethyl)-1-methylpyridinium iodide as described in Example 1 for 2-(o-nitrostyryl)-1-methylpyridinium iodide provides 2'-[2-(1-methyl-2-piperidyl)ethyl]formanilide which is purified by crystallization from isopropyl ether, (79% yield) m.p. 81°-84.5°C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931195 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-6bf78a4fb83d41d2873d5344272bb00c |
| Source note | uspto-grants-1976_01 |