HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 1-Ethyl-2-[2-(2-formamidophenyl)ethyl]pyridin-1-ium iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | HCID 20559958 | HCID 20559958 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-Ethyl-2-[2-(2-formamidophenyl)ethyl]pyridin-1-ium iodide | HCID 20560050 | — |
Reaction Steps
A solution of 2-(o-formamidophenethyl)pyridine (36.1 g., 0.159 mole) and iodoethane (30.0 g., 0.191 mole) in CH3CN (450 ml.) heated at reflux for 18 hr., cooled and diluted to incipient turbidity provides 1-ethyl-2-(o-formamidophenethyl)pyridinium iodide, yield, 44.8 g. (74%), m.p. 155°-157°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931195 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-30185de2a9ba46b4b79d564da43d65ea |
| Source note | uspto-grants-1976_01 |