HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzoyl chloride → 4-Bromo-2'-[2-(1-methyl-2-piperidyl)ethyl]benzanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzoyl chloride | HCID 68515 | — |
| Reactant | 2-(2-Aminophenethyl)-1-methylpiperidine | HCID 11085282 | — |
| Product | 4-Bromo-2'-[2-(1-methyl-2-piperidyl)ethyl]benzanilide | HCID 20559994 | — |
Reaction Steps
Reaction of 4-bromobenzoyl chloride with 2-(o-aminophenethyl)-1-methylpiperidine according to the procedure of Example 114 affords 4-bromo-2'-[2-(1-methyl-2-piperidyl)ethyl]benzanilide, m.p. 137.5°-138.5°C. (corr.), from ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931195 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-96dfccce2285471881ee7139ec1cd3f3 |
| Source note | uspto-grants-1976_01 |