Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3,4,5-Tetrahydropyridine → 2-Fluorenyl 2-pyrrolidinylmethyl ketone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3,4,5-Tetrahydropyridine | HCID 68161 | — |
| 반응물 | 2-Acetylfluorene | HCID 69908 | — |
| 반응물 | 1-Pyrroline | HCID 79803 | — |
| 반응물 | 2-Acetyldibenzofuran | HCID 293028 | — |
| 생성물 | 2-Fluorenyl 2-pyrrolidinylmethyl ketone | HCID 12300793 | — |
반응 단계
Following essentially the same procedure as in Example XI above, but substituting 2-acetylfluorene for the 2-acetyldibenzofuran above and substituting 1-pyrroline as the trimer for the 2,3,4,5-tetrahydropyridine (as α-tripiperidein) above results in the formation of 2-fluorenyl 2-pyrrolidinylmethyl ketone as the hydrochloride salt, and which when recrystallized from isopropyl alcohol has a M.P. of 234-44°C. (dec.)
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03931155 |
| 출처 데이터셋 | uspto-grants-1976_01 |
| ORD ID | ord-fb20cab4092b4b5e843807665404280b |
| 출처 메모 | uspto-grants-1976_01 |