HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethylformamide → 2-(2-Benzoylphenyl)-2-imidazoline
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethylformamide | HCID 6228 | — |
| Edukt | Sodium sulfite heptahydrate | HCID 160916 | — |
| Edukt | 2,3-dihydro-5-hydroperoxy-5-phenyl-5H-imidazo[2,1-a]isoindole | HCID 21439763 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 2-(2-Benzoylphenyl)-2-imidazoline | HCID 12406343 | — |
Reaktionsschritte
A solution of 0.7 g. of sodium sulfite heptahydrate in 3 ml. of water was added to 0.5 g. of 2,3-dihydro-5-hydroperoxy-5-phenyl-5H-imidazo[2,1-a]isoindole in 7 ml. of dimethylformamide. The solution was heated to 100° for 15 minutes. On cooling and addition of 20 ml. of water, 2-(2-benzoylphenyl)-2-imidazoline was obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US03931217 |
| Quelldatensatz | uspto-grants-1976_01 |
| ORD ID | ord-6a995959bfc34f67aa8778a57737b695 |
| Quellennotiz | uspto-grants-1976_01 |