HRID1579771

反应详情

EQUATION

反应方程式

HRID 1579771 的结构方程式

PROCEDURE

实验过程

20 g of m-benzoyl-phenyl acetic acid (prepared by process of French Pat. No. 1,546,478) and 100 ml of thionyl chloride were refluxed for 3 hours and then evaporated to dryness. Excess thionyl chloride was removed by entrainment with benzene to obtain 21.47 g of m-benzoyl-phenyl-acetic acid chloride.

WORKUP

后处理

  1. customevaporated to dryness
  2. customExcess thionyl chloride was removed by entrainment with benzene