HCID 23338077, compound → Methyldamascone

Participants

Reaction Steps

2,6,6-Trimethyl-1[1-hydroxy-3-methyl-2-butenyl]-1-cyclohexene, prepared according to Example 6, (1.0 g.) with activated MnO2 (10 g.) in 30 ml. of pentane was mixed at room temperature during 63 h. after filtration and distillation 630 mg. (63 %) of the desired ketone, B.p. 67°/0.001 Torr, were obtained.

Provenance & Evidence