反应详情

温度

50 °C

0.05 Mol of p-methyl benzyl chloride and 0.05 mol of sec.-butyl chloride were dissolved in 100 ml. of toluene. The solution obtained was added dropwise to a toluene solution containing 0.1 mol of potassium metal with thorough stirring while obtaining the temperature of the solution at 20° to 30°C. After the addition, the temperature of the solution was raised to 50°C. with thorough stirring to complete the reaction. After the reaction, the product became black violet, and a white powder was precipitated. The resultant product containing the unreacted matter and by-products was distilled to afford 3-methyl-4-(p-tolyl) butane. The resulting product was used in the following Examples.

1. customThe solution obtained
2. customwhile obtaining the temperature of the solution at 20° to 30°C
3. additionAfter the addition
4. stirringwith thorough stirring
5. customthe reaction
6. customAfter the reaction
7. customa white powder was precipitated
8. additionThe resultant product containing the unreacted matter and by-products
9. distillationwas distilled