HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminosalicylic Acid → HCID 12270306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminosalicylic Acid | HCID 4075 | — |
| Reactant | Cyclopentanone, 2-(2-oxo-2-phenylethyl)- | HCID 10655725 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12270306 | HCID 12270306 | — |
Reaction Steps
A mixture of 20.5 g. (0.1 mole) of 2-phenacylcyclopentanone, 15.3 g. (0.1 mole) of 5-aminosalicylic acid, and 60 ml. of glacial acetic acid was heated under reflux for 3 hours, cooled and filtered. The filter cake was washed with water, dried and recrystallized from acetic acid to provide 9.5 g. (30%) of crystals, m.p. 198°-199°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931407 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-59a359c8681e4358b9633df58d6b3c5a |
| Source note | uspto-grants-1976_01 |