HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Acetylamino)-5-aminobenzoic acid → HCID 12270277, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Acetylamino)-5-aminobenzoic acid | HCID 3016906 | — |
| Reactant | 2-(2-Oxo-2-phenylethyl)cyclohexanone | HCID 10512899 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 12270277 | HCID 12270277 | — |
Reaction Steps
A mixture of 11.7 g. (0.054 mole) of 2-phenacylcyclohexanone, 10.5 g. (0.054 mole) of 2-acetamido-5-aminobenzoic acid, and 50 ml. of glacial acetic acid was heated under reflux for 4 hours, cooled, diluted with 15 ml. of methanol and filtered. The collected solid was recrystallized from acetonitrile to provide 9.45 g. (47%) of crystals, m.p. 192° -194°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03931407 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-8fab6c3752f04c6ba5cb03cdbadfb81d |
| Source note | uspto-grants-1976_01 |