Ethanol → HCID 12270335, compound

HRID 1579903Notes

Reaction equation

HRID 1579903 reaction equation
N1([C:6]2[CH2:11][CH2:10][CH2:9][CH2:8][CH:7]=2)CCCC1.[N+:12]([C:15]1[CH:24]=[CH:23][C:18]([C:19](=[O:22])[CH2:20]Br)=[CH:17][CH:16]=1)([O-:14])=[O:13].C([OH:27])C>>[N+:12]([C:15]1[CH:24]=[CH:23][C:18]([C:19](=[O:22])[CH2:20][CH:7]2[CH2:8][CH2:9][CH2:10][CH2:11][C:6]2=[O:27])=[CH:17][CH:16]=1)([O-:14])=[O:13]

Participants

4

Reactant 3

HCID 702EthanolHCID 668402-Bromo-4'-nitroacetophenoneHCID 707681-Pyrrolidino-1-cyclohexene

Product 1

HCID 12270335HCID 12270335, compound

Procedure

(0.35 mole) of 1-pyrrolidino-1-cyclohexene and 85.0 g. (0.35 mole) of p-nitrophenacyl bromide by the method described in Example 39a gave 81.3 g. (89%) of crystals, m.p. 61°-63° (from ethanol).

Workup

  1. customgave 81.3 g

Sources & evidence

ORD record
ord-e44c8232aa2942de9ce2e5697528a25d
Source dataset
uspto-grants-1976_01
Patent number
US03931407

Reaction notes

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