HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichlorophenol → 2-(2,4-Dichlorophenoxy)-1-(4-methylphenyl)ethan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichlorophenol | HCID 8449 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chloro-1-(4-methylphenyl)ethan-1-one | HCID 237805 | — |
| Product | 2-(2,4-Dichlorophenoxy)-1-(4-methylphenyl)ethan-1-one | HCID 21496008 | — |
Reaction Steps
Following the procedure given in Example 13a 2,4-dichlorophenol was interacted with an equimolar quantity of 4-methylphenacyl chloride in the presence of potassium carbonate to give w-(2,4-dichlorophenoxy)-p-methylacetophenone. Recrystallized from 2-ethoxyethanol, this product melted at 96.5°-98.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932301 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-a5d2755ec2024488bd7957ed256a8730 |
| Source note | uspto-grants-1976_01 |