HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-(Dibenzo[b,d]furan-2-yloxy)-1-(p-tolyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Dibenzofuranol | HCID 66587 | — |
| Reactant | 2-Chloro-1-(4-methylphenyl)ethan-1-one | HCID 237805 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-(Dibenzo[b,d]furan-2-yloxy)-1-(p-tolyl)ethanone | HCID 21495975 | — |
Reaction Steps
Following the procedure given in Example 13a 2-hydroxydibenzofuran was interacted with 4-methylphenacylchloride in the presence of anhydrous potassium carbonate in acetone to give ω-(2-dibenzofuranyloxy)-p-methylacetophenone. Following recrystallization from 2-ethoxyethanol, this compound melted at 162°-164° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932301 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-c7ad5df5c6c445b58044c4519b50f253 |
| Source note | uspto-grants-1976_01 |