HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21564749, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 5-Hydroxy-1-tetralone | HCID 119921 | — |
| Reactant | 1-(3-Chloropropyl)-4-(2-methoxyphenyl)piperazine | HCID 622669 | — |
| Product | HCID 21564749 | HCID 21564749 | 78.8% |
Reaction Steps
from 5-hydroxy-1-oxotetraline and 1-(3-chloropropyl)-4-(2-methoxyphenyl)-piperazine; yield 78.8% of theory; the hydrochloride, after recrystallization from water and drying, contained 0.486 mol water; m.p. 174°-175°C;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932411 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-12b703771b9b4ab49a5b26d9a799327c |
| Source note | uspto-grants-1976_01 |