HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Hydroxy-1-tetralone → HCID 21564748, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Hydroxy-1-tetralone | HCID 119921 | — |
| Reactant | Tetrafluoro-m-phenylenediamine dihydrochloride | HCID 149026 | — |
| Reactant | 1-[(4-Chlorophenyl)methyl]-4-(3-chloropropyl)piperazine | HCID 13399727 | — |
| Product | HCID 21564748 | HCID 21564748 | 72.1% |
Reaction Steps
from 5-hydroxy-1-oxotetraline and 1-(3-chloropropyl)-4-(4-chlorobenzyl)-piperazine; yield 72.1% of theory; m.p. of the dihydrochloride (recrystallized from 1N hydrochloric acid) 239°C (decomposed);
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932411 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-4fa57106635b47dc9143a4d967a53a82 |
| Source note | uspto-grants-1976_01 |