Oxalyl chloride → HCID 13391839, compound

Participants

Reaction Conditions

Reaction Steps

260 ml of oxalyl chloride were added to 225 g of trichloroacrylamide in 525 ml of dichloroethane cooled to 2°C and the mixture was held at 0°C for 1 hour and then refluxed for 16 hours. The resulting solution was evaporated under reduced pressure and the residue was distilled to obtain 232 g of trichloroacryloyl-isocyanate boiling at 86°C under 20 mm Hg and having a refractive index nD23 = 1.538.

Provenance & Evidence