HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetonitrile → HCID 54476035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetonitrile | HCID 7856 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(dimethylamino)-2-hydroxybenzaldehyde | HCID 9815305 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 54476035 | HCID 54476035 | — |
Reaction Steps
82 parts of 4-dimethylaminosalicylaldehyde is dissolved in 500 parts by volume of acetone, then 96 parts of potassium carbonate and 45 parts of chloroacetonitrile are added and the whole is boiled under reflux for 10 hours. After the solution has been filtered it is concentrated and the crystals deposited are recrystallized from benzene with the addition of animal charcoal. 36 parts of colorless crystals of 2-formyl-5-dimethylaminophenoxyacetonitrile is obtained with a melting point of 124° to 125°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932446 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-9d1c6a998d93484390af7c4976fd287a |
| Source note | uspto-grants-1976_01 |