HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 131709906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Cyclobutanecarbonyl chloride | HCID 78705 | — |
| Reactant | HCID 131709901 | HCID 131709901 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 131709906 | HCID 131709906 | — |
Reaction Steps
5,5-Dimethyl-8-(4-p-fluorophenyl-1-methylbutyl)-10-hydroxy-1,2,3,4-tetrahydro-5H[1]benzopyrano[4,3-c]pyridin-10-ol (1 mole) and cyclobutanecarbonyl chloride (1 mole) with triethylamine (1 mole) in dimethylformamide, stirring 16 hours at 25°C gave the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03932432 |
| Source dataset | uspto-grants-1976_01 |
| ORD ID | ord-3871c442b67b446db8fae9542a08c4bd |
| Source note | uspto-grants-1976_01 |