Malononitrile → 2-Amino-6-chloro-4-oxo-4H-1-benzopyran-3-carbonitrile

HRID 1580185Notes

Reaction equation

HRID 1580185 reaction equation
C([O:4][C:5]1[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][C:6]=1[C:7](Cl)=[O:8])(=O)C.[C:15](#[N:19])[CH2:16][C:17]#[N:18]>>[NH2:18][C:17]1[O:4][C:5]2[CH:13]=[CH:12][C:11]([Cl:14])=[CH:10][C:6]=2[C:7](=[O:8])[C:16]=1[C:15]#[N:19]

Participants

3

Reactant 2

HCID 8010MalononitrileHCID 12196910HCID 12196910, compound

Product 1

HCID 214347342-Amino-6-chloro-4-oxo-4H-1-benzopyran-3-carbonitrile

Procedure

-- In the same way as described in Example 3, 2-acetoxy-5-chlorobenzoyl chloride and malononitrile are reacted to give crystals, mp 340°C.

Workup

  1. customare reacted
  2. customto give crystals, mp 340°C.

Sources & evidence

ORD record
ord-d9f0273d0f6f40bba875930a16f3f488
Source dataset
uspto-grants-1976_01
Patent number
US03932466

Reaction notes

Loading…