Malononitrile → HCID 21434737, compound

HRID 1580187Notes

Reaction equation

HRID 1580187 reaction equation
C([O:4][C:5]1[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][C:6]=1[C:7](Cl)=[O:8])(=O)C.[C:16](#[N:20])[CH2:17][C:18]#[N:19]>>[NH2:19][C:18]1[O:4][C:5]2[CH:13]=[CH:12][C:11]([O:14][CH3:15])=[CH:10][C:6]=2[C:7](=[O:8])[C:17]=1[C:16]#[N:20]

Participants

3

Reactant 2

HCID 8010MalononitrileHCID 12366435HCID 12366435, compound

Product 1

HCID 21434737HCID 21434737, compound

Procedure

In the same way as described in Example 3, 2-acetoxy-5-methoxy benzoyl-chloride and malononitrile are reacted to give crystals, mp 320°C after recrystallization from methanol.

Workup

  1. customare reacted
  2. customto give crystals, mp 320°C
  3. customafter recrystallization from methanol

Sources & evidence

ORD record
ord-4a59041b2d6f4fcab960898834f4bc80
Source dataset
uspto-grants-1976_01
Patent number
US03932466

Reaction notes

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